In present time there is an increasing need for an alternative material to conventional materials. Growing interest in using environmental friendly materials brings natural fiber made the composite material in focus. They are strong, lightweight, cheap and biodegradable. But one needs to check whether its properties satisfy that of existing material. The target of the study is to experimentally justify biaxial fiber composite as a promising alternate material. The polymer composite samples are made with natural/synthetic fiber as reinforcement and a synthetic resin as matrix material. To find its natural frequency and damping of the composite materials, vibration test is carried out. ANOVA technique is used to find the level of the parameter.